Please use this identifier to cite or link to this item: http://cmuir.cmu.ac.th/jspui/handle/6653943832/5030
Title: Analyses of nano-crystalline LiCoVO4 prepared by solvothermal reaction
Authors: Thongtem T.
Phuruangrat A.
Thongtem S.
Issue Date: 2006
Abstract: LiOH·H2O, Co(NO3)2·6H2O and NH4VO3 were used to prepare nano-crystalline LiCoVO4 by 150 °C solvothermal reaction in isopropanol for 10-360 h and subsequent calcination at 300-500 °C for 6 h. XRD, TEM and selected area electron diffraction (SAED) revealed the presence of nano-crystalline LiCoVO4 with inverse spinel structure. The V-O stretching vibration modes of VO4 tetrahedrons were detected by FTIR over the range 617-835 cm- 1 and by Raman spectrometer at 805.7 and 783.1 cm- 1. Co, V and O were detected by EDX. TGA of solvothermal products shows weight loss due to the evaporation and decomposition processes at 40-648 °C. © 2006 Elsevier B.V. All rights reserved.
URI: http://www.scopus.com/inward/record.url?eid=2-s2.0-33750284297&partnerID=40&md5=47a460be160b94ac9f725a3ac922322f
http://cmuir.cmu.ac.th/handle/6653943832/5030
ISSN: 0167577X
Appears in Collections:SCIENCE: Journal Articles

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